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Development of Hierarchically Porous Nickel Foam for Electrosynthesis of Value-added Chemicals

Title
Development of Hierarchically Porous Nickel Foam for Electrosynthesis of Value-added Chemicals
Author(s)
Wei Yi
DGIST Authors
Wei YiJiwoong YangJong-Sung Yu
Advisor
양지웅
Co-Advisor(s)
Jong-Sung Yu
Issued Date
2025
Awarded Date
2025-02-01
Type
Thesis
Description
Hierarchically porous nickel foam, electrocatalysis, value-added chemicals, high surface area, C-N coupling.
Table Of Contents
List of Contents

Abstract i
List of Contents iii
List of tables v
List of figures vi
Chapter 1. Background 1
1. Brief Introduction. 1
Chapter 2: High Faradaic Efficiency Electrosynthesis of Benzimidazoles by C-N Coupling of Diamines
and CO2 on Cu Nanoparticles Coated on a Novel Hierarchically Porous Nickel Foam 3
2.1 Introduction 3
2.2. Experimental sections 5
2.3 Results and discussions 9
2.3.1 Characterizations of hNiF 9
2.3.2. Characterizations of Cu NPs coated hNiF. 12
2.3.3. Electrochemical performance of the prepared catalysts. 15
2.3.4. C-N coupling reaction mechanism analysis 20
2.4. Conclusion 25
Chapter 3. Formamide Electrosynthesis from Ammonia and Methanol over Noble-Metal Nanoparticles
Modified Hierarchically Porous Nickel Foam 26
3.1 Background. 26
3.2. Experimental section 28
3.3 Results and discussions 30
3.4. Conclusion 40
Chapter 4. Electrocatalytic Anodic Hydrogen Evolution and Formate Production on Cu/CuOx Coated on
Hierarchically Porous Nickel Foam 41
4.1 Background 41
4.2 Materials and Methods 44
4.3. Results and discussions 48
4.4. Conclusion 64
References 66
Chapter 5. Summarization 77
요 약 문 79
URI
http://hdl.handle.net/20.500.11750/57979
http://dgist.dcollection.net/common/orgView/200000843357
DOI
10.22677/THESIS.200000843357
Degree
Doctor
Department
Department of Energy Science and Engineering
Publisher
DGIST
Related Researcher
  • 양지웅 Yang, Jiwoong
  • Research Interests Quantum Dots; Nanocrystals; Displays; Solar Energy; TEM; Photocatalyst
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Department of Energy Science and Engineering Theses Ph.D.

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